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Fabrication of nano-network gold films via anodization of gold electrode and their application in SERS
Authors:Yingchang Yang  Yue Xia  Wei Huang  Jufang Zheng  Zelin Li
Affiliation:(1) Key Laboratory of Chemical Biology and Traditional Chinese Medicine Research (Ministry of Education of China), College of Chemistry and Chemical Engineering, Hunan Normal University, Lushan Road, Changsha, 410081, China;(2) Key Laboratory of the Ministry of Education for Advanced Catalysis Materials, Institute of Physical Chemistry, Zhejiang Normal University, Jinhua, 321004, China;
Abstract:We report here a green and facile one-step method to fabricate nano-network gold films of low roughness via anodization of gold electrodes in an aqueous solution of l-ascorbic acid (AA) or hydroquinone (H2Q) at the oxidation peak potential. The preparation involves the formation of thin gold oxide layer by anodization of gold and its simultaneous and/or subsequent reduction by AA or H2Q. The as-fabricated nano-network gold films show very strong SERS activity in comparison with the substrates prepared by some other electrochemical roughening methods.
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