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| 一种改进的SPME方法提取火场残留物中的促燃剂 | |
| 引用本文： | 何洪源,朱丹,张淑芳,陈占合.一种改进的SPME方法提取火场残留物中的促燃剂[J].分析试验室,2008,27(7). |
| 作者姓名： | 何洪源 朱丹 张淑芳 陈占合 |
| 作者单位： | 1. 中国人民公安大学刑科技系,北京,100038 2. 天津市公安局,天津,300040 3. 北京市公安局刑科所,北京,100054 |
| 基金项目： | 公安大学院士基金 , 北京市教委共建项目 |
| 摘 要： | 对当前国内外用于火场残留物中促燃剂的提取方法进行研究,包括采用活性炭片法(ACS)、固相微萃取(SPME)以及对固相微萃取技术从传统的热解吸模式到溶剂脱附模式的扩展性思考。通过提取3种促燃剂(汽油,煤油和柴油)检材的效能比较与分析,优化了实验条件,确定了SPME的提取和溶剂脱附的方法,实验研究表明,SPME-溶剂脱附法是火场促燃剂残留物分析的有效方法之一。 |
| 关 键 词： | 火场残留物 促燃剂 固相微萃取 |
Extraction of accelerants in fire debris by an improved SPME method |
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| HE Hong-yuan,ZHU Dan,ZHANG Shu-fang,CHEN Zhan-he.Extraction of accelerants in fire debris by an improved SPME method[J].Chinese Journal of Analysis Laboratory,2008,27(7). | |
| Authors: | HE Hong-yuan ZHU Dan ZHANG Shu-fang CHEN Zhan-he |
| Abstract: | Based on the research at home and abroad,an expansion of SPME sampling from thermal desorption mode to solvent-based desorption for the analysis of ignitable debris were described.Relied on the comparison of results between the two modes for testing three ignitable liquids(gasoline,kerosene,and diesel fuel),the experiment conditions were optimized and the detailed method of SPME extraction and solvent-based desorption in this paper were established.The results showed solvent-based desorption SPME was one of the effective methods to analyze the accelerants in fire debris. |
| Keywords: | Fire debris Accelerant SPME |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ | |