| 气相色谱－质谱联用等技术鉴定四氯化碳生产中固体堵塞物 |
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| 引用本文： | 孙定一,程超仁,王宏磊,李开生. 气相色谱－质谱联用等技术鉴定四氯化碳生产中固体堵塞物[J]. 色谱, 1994, 0(4) |
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| 作者姓名： | 孙定一 程超仁 王宏磊 李开生 |
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| 作者单位： | 河南省化学研究所，郑州农药厂，河南省卫生防疫站，河南省产品质量监督检验所 |
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| 摘 要： | 本文采用气相色谱联用等技术，对ＣＣｌ＿４生产中的固体堵塞物进行了剖析。该固体堵塞物的主要成分和含量为：六氯苯，９８．６４％；其次还有１，１，２，３，４，４－六氯－１，３－丁二烯和１，２，３，４，５，５－六氯－１，３－环戊二烯。
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| 关 键 词： | 气相色谱－质谱，气－液色谱，四氯化碳，六氯苯，核磁共振谱，红外光谱 |
Study on the Chemlcal Constituents of the Solid Blocks Formed in the Productlon of CCl_4 by Gas Chromatography-Mass Spectrometry(GC-MS) |
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| Sun Dingyi, Cheng Chaoren, Wang Honglei, and Li Kaisheng. Study on the Chemlcal Constituents of the Solid Blocks Formed in the Productlon of CCl_4 by Gas Chromatography-Mass Spectrometry(GC-MS)[J]. Chinese journal of chromatography, 1994, 0(4) |
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| Authors: | Sun Dingyi Cheng Chaoren Wang Honglei Li Kaisheng |
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| Abstract: | n This paper,the chemical constituents of the solid blocks formed in the pipe-line for the production ofCCl_4 have been analysed by GC-MS.The majority of them is hexachlorobenzene(89.14%)and others are l,1,2,3,4,4-hexachloro-l,3-butadiene and l,2,3,4,5-hexachloro-l,3-cyclopentadiene |
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| Keywords: | gas-liquid chromatography gas chromatography-mass spectrometry hexachlorobenzene CCl_4 nuclear magnetic resonance spectrometry infrared spectrometry |
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