| 气质联用单离子监测法测定纺织品中1-萘胺和2-萘胺 |
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| 引用本文： | 张伟亚,刘丽,唐丽纯,李英.气质联用单离子监测法测定纺织品中1-萘胺和2-萘胺[J].分析试验室,2003,22(3):68-70. |
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| 作者姓名： | 张伟亚 刘丽 唐丽纯 李英 |
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| 作者单位： | 深圳出入境检验检疫局,深圳,518045 |
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| 摘 要： | 采用气质联用单离子监测法(SIM)测定纺织品中1-萘胺和2-萘胺，对提取条件进行了优化，采用保留时间和全扫描质谱图定性，特征离子m/z143为监测离子，以其峰面积定量。
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| 关 键 词： | 单离子监测法 测定 纺织品 1－萘胺 2－萘胺 偶氮染料 气相色谱／质谱联用技术 |
| 文章编号： | 1000-0720(2003)03-0068-03 |
Determination of 1-naphthalenamine and 2-naphthalenamine in textiles by single ion monitoring method |
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| ZHANG Wei-ya,LIU Li,TANG Li-chun and LI Ying.Determination of 1-naphthalenamine and 2-naphthalenamine in textiles by single ion monitoring method[J].Chinese Journal of Analysis Laboratory,2003,22(3):68-70. |
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| Authors: | ZHANG Wei-ya LIU Li TANG Li-chun and LI Ying |
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| Abstract: | A new method for determination of 1-naphthalenamine and 2-naphthalenamine in textile samples by gas chromatography/mass spectrometry/single ion monitoring was developed. Several preparation methods were compared. Retention time and mass spectra of total ion chromatography were used for determination. The m/z 143 was quantitative ion for 1-naphthalenamine and 2-naphthalenamine. |
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| Keywords: | Textile SIM 1-naphthalenamine 2-naphthalenamine |
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