Synthesis and Crystal Structure of New Heterocyclic Compounds Containing 1,2,3-Triazole Moiety |
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Authors: | Zhi-Qiang Dong Fang-Ming Liu Yong-Ming Zeng |
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Institution: | (1) College of Materials and Chemical Engineering, Hangzhou Normal University, Hangzhou, 310036, People’s Republic of China;(2) College of Chemistry and Chemical Engineering, Xinjiang University, Urumqi, 830046, People’s Republic of China; |
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Abstract: | Abstract A series of new heterocyclic compounds bearing 1,2,3-triazole moiety were synthesized using 4-acetyl-2-phenyl-1,2,3-triazole
1 as the starting material. The target compounds were prepared and the structures were characterized by IR, 1H NMR, MS and elemental analysis. Meanwhile, the crystal structures of the synthesized compounds were also furthered confirmed
by X-ray diffraction analysis. Compound 3b crystallized in the monoclinic P2(1)/c space group with unit cell parameters a = 10.6974(17) ?, b = 20.356(3) ?, c = 7.8049(12) ?, α = 90°, β = 102.840(3)°, γ = 90o,
V = 1657.1(5) ?3, Z = 4, T = 293(2) K. Compound 7c crystallized in the Triclinic P-1 space group with unit cell parameters a = 7.364(2) ?, b = 7.366(2) ?, c = 26.089(8)?, α = 87.114(7)°, β = 87.040(7) (3)°,
γ = 82.337(7)°, V = 1399.2(7) ?3, Z = 2, T = 293(2) K. Compound 10c crystallized in the Triclinic P-1 space group with unit cell parameters a = 9.8152(10) ?, b = 10.0806(13) ?, c = 11.1267(14) ?, α = 100.344(3)°, β = 111.975(3)°,
γ = 107.852(3)°, V = 916.18(19) ?3, Z = 2, T = 293(2) K. |
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