Reaction of 3-methoxy-2-methylphenol with 2-ethoxyvinylphosphonic dichloride |
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| Authors: | Yu M Sadykova N V Dalmatova A R Burilov M A Pudovik A B Dobrynin |
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| Institution: | 1. A. E. Arbuzov Institute of Organic and Physical Chemistry Kazan Scientific Center of the Russian Academy of Sciences, 8 ul. Akad. Arbuzova, 420088, Kazan, Russian Federation
2. Kazan State Technological University, 68 ul. K. Marksa, 420015, Kazan, Russian Federation
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| Abstract: | Condensation of 2-ethoxyvinylphosphonic dichloride with 3-methoxy-2-methylphenol in dioxane in the presence of trifluoroacetic acid results in 5,13-dimethoxy-4,14-dimethyl-1-phospha-2,16-dioxatetracyclo7.7.1.03,8.010,15]heptadeca-3,5,7,10,12,14-hexaene 1-oxide and 2-hydroxy-7-methoxy-8-methyl-2-oxobenzoe]-1,2-oxophosphorine. |
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