| SO42-/Al-MCM-41介孔分子筛合成与表征 |
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| 引用本文： | 邢凤兰,吴平,王清滨.SO42-/Al-MCM-41介孔分子筛合成与表征[J].齐齐哈尔大学学报(自然科学版),2006,22(6):1-3. |
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| 作者姓名： | 邢凤兰 吴平 王清滨 |
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| 作者单位： | 齐齐哈尔大学化学与化学工程学院,黑龙江,齐齐哈尔,161006 |
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| 摘 要： | 采用十六烷基三甲基溴化铵作为模板剂,正硅酸乙酯为硅源,铝酸钠为铝源,用水热晶化法在乙二胺为碱性介质中合成了n(Si):n(Al)=50:1的Al-MCM-41介孔分子筛,并用浸渍法制备SO42-/Al-MCM-41。通过XRD、氮气吸附-脱附、Hammett指示剂胺滴定等方法对所合成样品进行表征。
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| 关 键 词： | 介孔分子筛 合成 |
| 文章编号： | 1007-984X(2006)06-0001-03 |
| 收稿时间： | 2006-09-15 |
| 修稿时间： | 2006年9月15日 |
Synthesis, characterization of SO42-/Al-MCM-41 mesoporous molecular |
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| XING Feng-lan,Wu Ping,WANG Qing-bin.Synthesis, characterization of SO42-/Al-MCM-41 mesoporous molecular[J].Journal of Qiqihar University(Natural Science Edition),2006,22(6):1-3. |
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| Authors: | XING Feng-lan Wu Ping WANG Qing-bin |
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| Institution: | CoUege of Chemistry and Chemical Engineering of Qiqihar University, Heilongjiang Qiqihar 161006,China |
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| Abstract: | The mesoporous molecular sieves Al-MCM-41 is synthesized under hydrothermal condition using cetyl trimethyl ammonium bromide(CTAB) surfactants as template,tetraetylorthosilicate(TEOS)as silicic,sodium aluminate as aluminum source,according to the ratio of Si:Al =50:1.0.SO42-/Al-MCM-41 mesoporous molecular sieves was obtained with sulfuric acid by infusing.Al-MCM-41 and SO42-/Al-MCM-41 are characterized by power X-ray diffraction(XRD),nitrogen adsorption and Hammett measurements. |
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| Keywords: | SO42-/Al-MCM-41 |
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