Synthesis and Crystal Structure of [2-(4-chlorobenzoyloxy)-5-methylphenyl]-(4-methylphenyl)methanone期刊界 All Journals 搜尽天下杂志传播学术成果专业期刊搜索期刊信息化学术搜索

Synthesis and Crystal Structure of [2-(4-chlorobenzoyloxy)-5-methylphenyl]-(4-methylphenyl)methanone

Authors:	S. Naveen T. D. Venu S. Shashikanth M. A. Sridhar J. Shashidhara Prasad

Affiliation:	(1) Department of Studies in Physics, University of Mysore, Manasagangotri, Mysore, 570 006, India;(2) Department of Studies in Chemistry, University of Mysore, Mysore, 570 006, India

Abstract:	[2-(4-Chlorobenzoyloxy)-5-methylphenyl]-(4-methylphenyl)methanone was synthesized and characterized by spectroscopic and X-ray diffraction methods. The molecule crystallizes in the monoclinic space group P2₁/c with cell parameters a = 13.7530(19) Å, b = 10.0560(19) Å, c = 13.469(3) Å, β = 100.630(7)° and Z = 4. There is a large discrepancy between the carbonyl group bond lengths of ketone and the ester. The structure exhibits intermolecular hydrogen bonds of the type C–H···O.

Keywords:	Benzophenones Crystal structure Hydrogen bond
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