The structures of 2-(4,5-dihydro-5-aryl-3-isoxazolyl)-1-arylethanone oximes. An unusual behaviour in its 1H-NMR and mass spectra |
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Authors: | Eduardo Díaz Hctor Barrios Rubn A Toscano Francisco Yuste William F Reynolds Jos Luis Aguilera Efrn Caballero |
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Institution: | Eduardo Díaz,Héctor Barrios,Rubén A. Toscano,Francisco Yuste,William F. Reynolds,José Luis Aguilera,Efrén Caballero |
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Abstract: | The reaction of dibenzalacetones substituted on the aromatic ring with hydroxylamine hydrochloride and potassium hydroxide in refluxing ethanol affords several compounds. Herein, we report the structures and spectral properties of several oximes of 2-(4,5-dihydro-5-aryl-3-isoxazolyl)-1-arylethanones 6 . Unusual behaviour on its 1H-nmr and mass spectra was observed. Single crystal X-ray diffraction was performed on compound 6d to support our structural considerations abouth the title compounds. |
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