Characterization of modified glassy carbon films |
| |
| Authors: | Falko Schlottig Joachim Schreckenbach Klaus Witke Günter Marx |
| |
| Institution: | (1) Institut für Chemie, Technische Universität Chemnitz-Zwickau, D-09107 Chemnitz, Federal Republic of Germany;(2) Bundesanstalt für Materialforschung und -prüfung Berlin, Federal Republic of Germany |
| |
| Abstract: | The composition and structure of the thin conversion films at pre- and breakdown state are investigated. The breakdown leads to a modified structure and composition. Raman spectra of modified films show the formation of glassy carbon with a defined size of crystallites. A typical morphology characterized by a strong structured surface indicates this breakdown state. Electron diffraction patterns of the pre-breakdown state show the presence of titanium nitride, titanium carbide and titanium oxide.Dedicated to Professor Dr. rer. nat. Dr. h.c. Hubertus Nickel on the occasion of his 65th birthday |
| |
| Keywords: | glassy carbon Raman SEM acetonitrile titanium |
| 本文献已被 SpringerLink 等数据库收录！ |
