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碘解磷定的ICP-AES测定
引用本文:王伟.碘解磷定的ICP-AES测定[J].光谱实验室,2002,19(2):264-266.
作者姓名:王伟
作者单位:盐城工学院化工系,江苏省盐城市黄海中路20号,224003
摘    要:利用等离子体发射光谱法间接碘解磷。在pH5.0的溶液中,当四苯硼钠过量时可完全沉淀碘解磷定,测定滤液中剩余的四苯硼钠,使可计算得到碘解磷定的含量。该方法简单、快速,回收率在97%-101%之间,相对标准偏差小于2.1%。

关 键 词:电感耦合等离子体-原子发射光谱  碘解磷定  四苯硼钠  沉淀  解毒药  药物分析
文章编号:1004-8138(2002)02-0264-03
修稿时间:2001年12月6日

Determination of Pralidoximi Iodidum by ICP-AES
WANG Wei.Determination of Pralidoximi Iodidum by ICP-AES[J].Chinese Journal of Spectroscopy Laboratory,2002,19(2):264-266.
Authors:WANG Wei
Abstract:The method for indirect determination of pralidoximi iodidum by inductively coupled plasma atomic emission spectroscopy (ICP AES) was studied.In the solution of pH5.0,the pralidoximi iodidum was completely precipitated by excessive sodium tetraphenylborate. The boron in filtrate was detected by ICP AES for calculating the content of pralidoximi iodidum. The average recovery was in the range of 97%-101% and RSD was less than 2.1%.
Keywords:Inductively Coupled Plasma  Atomic Emission Spectroscopy  Pralidoximi Iodidum  Sodium Tetraphenylborate  Precipitation  
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