| Crystal Structure of 3－［（α－Phenyl） triphenyl germylethyl］－4－phenyl－Δ~2－1，2，4－triazoline－5－thione |
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| 引用本文： | Chen Ru-Yu, Li Feng-Fu (Institute of Elemento-Organic Chemistry,Hankai University,Tianjin,300071). Crystal Structure of 3－［（α－Phenyl） triphenyl germylethyl］－4－phenyl－Δ~2－1，2，4－triazoline－5－thione[J]. 结构化学, 1995, 0(4) |
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| 作者姓名： | Chen Ru-Yu Li Feng-Fu (Institute of Elemento-Organic Chemistry Hankai University Tianjin 300071) |
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| 作者单位： | Institute of Elemento-Organic Chemistry，Hankai University，Tianjin，300071 |
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| 摘 要： | ＣｒｙｓｔａｌＳｔｒｕｃｔｕｒｅｏｆ３－［（α－Ｐｈｅｎｙｌ）ｔｒｉｐｈｅｎｙｌｇｅｒｍｙｌｅｔｈｙｌ］－４－ｐｈｅｎｙｌ－Δ~２－１，２，４－ｔｒｉａｚｏｌｉｎｅ－５－ｔｈｉｏｎｅＣｈｅｎＲｕ－Ｙｕ；ＬｉＦｅｎｇ－Ｆｕ（ＩｎｓｔｉｔｕｔｅｏｆＥｌｅ?..
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Crystal Structure of 3-[(α-Phenyl) triphenyl germylethyl]-4-phenyl -Δ￣2-1, 2, 4-triazoline-5-thione |
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| Chen Ru-Yu, Li Feng-Fu. Crystal Structure of 3-[(α-Phenyl) triphenyl germylethyl]-4-phenyl -Δ￣2-1, 2, 4-triazoline-5-thione[J]. Chinese Journal of Structural Chemistry, 1995, 0(4) |
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| Authors: | Chen Ru-Yu Li Feng-Fu |
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| Abstract: | The crystal structure of the title compound, C_34H_29GeN_3S, has been determined by single-crystal X-ray diffraction at 299 (±1)K. The crystal is trichlnic with space group P1, a=9. 772(3), b= 11. 643(3), c= 13. 960(3) A . α=66. 55(2),β=83. 49(2),γ=88. 49(2)°, Z=2, V= 1440. 0(8) A￣3, M_r=584. 28, F(000) =604, μ(MoKα) = 11. 44 cm￣-1. D_c= l. 349 g/cm￣-3. The final R factor is 0. 058, and R_w is 0. 068. The result of X-ray analysis indicates that the heterocycle of the title compound appears as a triazoline instead of a triazole. |
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| Keywords: | trizoline heterocycle organogermanium crystal structure |
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