Calculation of Kinetic Parameters for Crystallization Processes |
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Authors: | Isaac Asencio Fernando Dorado Paula Sánchez Justo Lobato |
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Institution: | (1) Department of Chemical Engineering, University of Castilla-La Mancha. Campus Universitario, s/n 13004, Ciudad Real, Spain |
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Abstract: | In this work, kinetic data of crystallization processes have been determined by measurement of the intensities of reflection of X-ray diffraction spectra and modeled using the Avrami-Eroféev and Jander expressions. We have created a simple Microsoft Excel spreadsheet that allows students to calculate the kinetic data. Students will be able to calculate the kinetic parameters of any crystallization process, for example, hydrothermal crystallization of catalytic materials like zeolites. The possibility of using the spreadsheet with different models or expressions and discriminating among them is also validated by comparing the model results with experimental data (differential thermal analyses, DTA) from papers available in the recent literature. |
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