The triethyl ammonium salt of O,O′-bis(o-tolyl) dithiophosphate [Et3NH]+[(2-MeC6H4O)2PS2]? |
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| Authors: | J. E. Drake C. L. B. MacDonald A. Kumar S. K. Pandey R. Ratnani |
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| Affiliation: | (1) Department of Chemistry and Biochemistry, University of Windsor, Windsor, Ontario, N9B 3P4, Canada;(2) Department of Chemistry, Jammu University, Jammu, 180 006, India;(3) Department of Pure & Applied Chemistry, M.D.S. University, Ajmer, 305 009, India |
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| Abstract: | The X-ray structure of the triethyl ammonium salt of O,O′-bis(o-tolyl)dithiophosphate, [Et3NH]+[(2-MeC6H4O)2PS2]−, has been determined. Crystal data: Monoclinic, P21/c, a = 15.4342(6) Å, b = 10.1913(4) Å, c = 14.0729(6) Å, β = 100.855(1)∘, V = 2174.0(2) Å−3, Z = 4. The immediate environment around phosphorous is distorted tetrahedral with two sulfur and two oxygen atoms in the coordination sphere, with N–H–S bonding involving only one of the sulfur atoms. |
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| Keywords: | Synthesis structure cresol tolyl dithiophosphate |
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