| Synthesis, Crystal Structure and Antibacterial Activities of 3-[3-Methyl-（2-thienyl）methyl-enehydrazinocarbonyl]-（1H）-1,2,4-triazole |
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| 引用本文： | YANG Jian-Guoa PAN Fu-Youb② SHAO Hongb,a.Synthesis, Crystal Structure and Antibacterial Activities of 3-[3-Methyl-（2-thienyl）methyl-enehydrazinocarbonyl]-（1H）-1,2,4-triazole[J].结构化学,2005,24(11):1286-1289. |
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| 作者姓名： | YANG Jian-Guoa PAN Fu-Youb② SHAO Hongb a |
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| 作者单位： | YANG Jian-Guoa PAN Fu-Youb② SHAO Hongb a (Office of Assets Administration，Taizhou University，Zhejiang 317000，China) b (Department of Chemistry，Taizhou University，Zhejiang 317000，China) |
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| 基金项目： | This work was supported by the Natural Science Foundation of Zhejiang Province (No. M203115) and Scientific Research Fund of Zhejiang Provincial Education Department(NO.20050057) |
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| 摘 要： | 1 INTRODUCTION Azole derivatives, such as the derivatives of pyra- zole, imidazole, triazole including benzotriazole, te- trazole and indole, have extensive biological activi- ties. They have become the central focus of studies of agricultural chemicals, medicines, plant growth regulating agents and so on1, 2]. Schiff bases also constitute a good type of biologically active sub- structures. Studies on pyrazole Schiff base-type fun- gicides have been reported3, 4]. However, some struc- …
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| 关 键 词： | 三唑 合成方法 晶体结构 抗菌活性 衍生物 |
Synthesis, Crystal Structure and Antibacterial Activities of 3-[3-Methyl-(2-thienyl)methyl-enehydrazinocarbonyl]-(1H)-1,2,4-triazole |
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| YANG Jian-Guo,PAN Fu-You,SHAO Hong.Synthesis, Crystal Structure and Antibacterial Activities of 3-[3-Methyl-(2-thienyl)methyl-enehydrazinocarbonyl]-(1H)-1,2,4-triazole[J].Chinese Journal of Structural Chemistry,2005,24(11):1286-1289. |
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| Authors: | YANG Jian-Guo PAN Fu-You SHAO Hong |
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| Institution: | 1. Office of Assets Administration, Taizhou University, Zhejiang 317000, China
2. Department of Chemistry, Taizhou University, Zhejiang 317000, China |
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| Abstract: | The title compound, C9HgN5OS, was synthesized by the reaction of 3-(1H)-1,2,4-triazole hydrazine with 3-methyl-2-thiophenecarboxaldehyde in ethanol. The single crystal structure has been determined by X-ray diffraction analysis. The crystal belongs to monoclinic system,space group P21/n with a = 9.5550(10), b = 11.9847(12), c = 10.1074(11) A, β= 112.995(2)°, V=1065.47(19) A3, Z = 4, μ = 0.290 mm-1, Mr= 235.27, Dc = 1.467 g/cm3 and F(000) = 488. The structure was solved by direct methods and refined to R = 0.0449. The crystal structure involves certain antibacterial activity. |
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| Keywords: | synthesis crystal structure antibacterial activities (1H)-1 2 4-triazole |
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