A facile route to perylenequinone |
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Institution: | 1. Institute Center for Water and Environment (iWATER), Department of Mechanical and Materials Engineering, Masdar Institute of Science and Technology, Abu Dhabi 54224, United Arab Emirates;2. MAScIR Foundation, VARENA Center, Rabat Design, Rue Mohamed El Jazouli, Madinat Al Irfane, Rabat 10100, Morocco;3. Institute Center for Energy (iENERGY), Department of Mechanical and Materials Engineering, Masdar Institute of Science and Technology, Abu Dhabi 54224, United Arab Emirates;1. Organic Chemistry Division, National Chemical Laboratory (CSIR-NCL), Dr. Homi Bhabha Road, Pashan, Pune 411008, India;2. Physical & Materials Chemistry Division, CSIR-National Chemical Laboratory, Dr. Homi Bhabha Road, Pune 411008, Maharashtra, India;1. Department of Pharmaceutical Organic Chemistry, College of Pharmacy, Al-Azhar University, Cairo, 11884, Egypt;2. Department of Comparative Pathobiology, College of Veterinary Medicine, Purdue University, West Lafayette, IN, 47907, USA;3. Purdue Institute of Inflammation, Immunology, and Infectious Disease, West Lafayette, IN, 47907, USA;4. University of Science and Technology, Nanoscience Program, Zewail City of Science and Technology, October Gardens, 6th of October, Giza, 12578, Egypt;1. College of Chemistry & Chemical Engineering, Shaanxi Key Laboratory of Chemical Additives for Industry, Shaanxi University of Science & Technology, Xi’an, Shaanxi, 710021, China;2. Xi''an Aeronautical Polytechnic Institute, Xi’an, Shaanxi, 710089, China;3. School of Chemistry & Chemical Engineering, Shaanxi Normal University, Xi’an, Shaanxi, 710119, China;4. Shaanxi Key Laboratory of Comprehensive Utilization of Tailings Resources, College of Chemical Engineering and Modern Materials, Shangluo University, Shangluo, Shaanxi, 726000, China |
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Abstract: | Two-stage Ullmann and phenol coupling were effected in a singleoperation on methyl 5-bromo-1,2-dihydroxy-6,8-dimethoxynaphthalene-3-acetate to give dimethyl 5,8-dihydroxy-1,3,10,12-tetramethoxy-4,9-perylenequinone-6,7-diacetatewith ferric chloride as oxidant. |
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