Reactions of nitrosonium hexafluorophosphate with some olefinic compounds in acetonitrile: one step synthesis of 4H-5,6-dihydro-1,2-oxazines |
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| Affiliation: | 1. Department of Chemistry, Biochemistry Division, University of Florida, Gainesville, FL 32611, USA;2. Department of Pharmacology and Therapeutics, University of Florida, College of Medicine, Gainesville, FL 32610, USA;1. School of Chemistry and Chemical Engineering, Shanxi University, Taiyuan, 030006, PR China;2. Institute of Molecular Science, Chemical Biology and Molecular Engineering, Laboratory of Education Ministry, Shanxi University, Taiyuan 030006, PR China;1. Department of Medical Bioengineering, Okayama University, 3-1-1 Tsushimanaka, Okayama 700-8530, Japan;2. Department of Applied Chemistry, Kindai University, 3-4-1 Kowakae, Higashi-Osaka, Osaka 577-8502, Japan;3. Institute of Advanced Energy, Kyoto University, Gokasho, Uji, Kyoto 611-0011, Japan;4. Department of Applied Chemistry, Osaka Prefecture University, 1-1 Gakuen-cho, Naka-ku, Sakai, Osaka, Japan;1. Institut de Science des Matériaux de Mulhouse IS2M, UMR CNRS 7361, UHA, 15, rue Jean Starcky, 68057 Mulhouse Cedex, France;2. Aix-Marseille Université, CNRS, Institut de Chimie Radicalaire ICR, UMR 7273, 13397 Marseille, France;3. Department of Chemical Engineering and Waterloo Institute for Nanotechnology (WIN), University of Waterloo, 200 University Ave West, Waterloo, Ont. N2L 3G1, Canada;1. Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences, Leninskii pr. 31, Moscow 119991, Russia;2. Moscow Technological University, pr. Vernadskogo 86, Moscow 119571, Russia;3. Mendeleev University of Chemical Technology of Russia, Miusskaya pl. 9, Moscow 125047, Russia |
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| Abstract: | Reactions of nitrosonium hexafluorophosphate or tetrafluoroborate with olefins having aryl groups at an olefinic carbon atom at low temperature in acetonitrile afforded 4H-5,6-dihydro-1,2-oxazines with two aryl groups at C-4 and C-6 in fair to good yields. |
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