| 4,4＇-二硝基二苯乙烷(烯)的合成 |
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| 引用本文： | 卢俊瑞,王亚林,冯燕,顾玲. 4,4＇-二硝基二苯乙烷(烯)的合成[J]. 应用化学, 2000, 17(6): 651-0 |
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| 作者姓名： | 卢俊瑞 王亚林 冯燕 顾玲 |
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| 作者单位： | 天津理工学院，天津职工化工学院 |
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| 基金项目： | 天津市 2 1世纪青年科学基金资助项目!(97370 16 11) |
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| 摘 要： | 二硝基二苯乙烯;硝基甲苯;氧化二聚反应;4;4＇-二硝基二苯乙烷(烯)的合成
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| 关 键 词： | 二硝基二苯乙烯 硝基甲苯 氧化二聚反应 4’-二硝基二苯乙烷(烯)的合成 |
| 收稿时间： | 2009-06-29 |
| 修稿时间： | 2009-06-29 |
Synthesis of 4,4'-Dinitrodibenzyl and 4,4'-Dinitrostilbene |
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| LU Jun-Rui,WANG Ya-Lin,FENG Yan,GU Ling. Synthesis of 4,4'-Dinitrodibenzyl and 4,4'-Dinitrostilbene[J]. Chinese Journal of Applied Chemistry, 2000, 17(6): 651-0 |
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| Authors: | LU Jun-Rui WANG Ya-Lin FENG Yan GU Ling |
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| Abstract: | The title compounds were synthesized by oxidative dimerization of p-nitrotoluene. The effects of solvents, bases and oxidizing agents on the dimerization were investigated. The results showed that by selecting appropriate solvents, oxidizing agents, base catalysts and controlling technical conditions the yields of dinitrodibenzyl and dinitrostilbene could be reached 89.4% and 74.6%, respectively. |
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| Keywords: | dinitrobenzyl dinitrostilbene synthesis nitrotoluene oxidative dimerization8 |
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