Synthesis and crystal structure of 1,1,1,5,5,5-hexafluoro-2-aminopentan-4-one (HFAP)期刊界 All Journals 搜尽天下杂志传播学术成果专业期刊搜索期刊信息化学术搜索

Synthesis and crystal structure of 1,1,1,5,5,5-hexafluoro-2-aminopentan-4-one (HFAP)

Authors:	D.A. Johnson A.B. Waugh T.W. Hambley J.C. Taylor

Affiliation:	Division of Energy Chemistry, CSIRO, Lucas Heights Research Laboratories, Private Mail Bag 7, Sutherland, NSW, 2232 Australia

Abstract:	The vapour phase reaction of ammonia and hexafluoroacetylacetone leads to the formation of the new β-keto-amine C₅H₃F₆NO. Crystals of the compound are monoclinic, space group $P$ 2₁/ $n$ , $a$ = 10.01(2), $b$ = 19.33(3), $c$ = 8.40(1) Å, β = 82.27(6)°; final R = 0.044.

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