| Meso-四(对烷氧苯基)卟啉金属银配合物的激光解吸电离飞行时间质谱表征 |
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| 引用本文： | 季怡萍,张红明,刘子阳.Meso-四(对烷氧苯基)卟啉金属银配合物的激光解吸电离飞行时间质谱表征[J].分析测试技术与仪器,2006,12(3):158-160. |
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| 作者姓名： | 季怡萍 张红明 刘子阳 |
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| 作者单位： | 1. 中国科学院,长春应用化学研究所,吉林,长春,130022
2. 浙江大学,化学系,淅江,杭州,310027 |
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| 摘 要： | 通过激光解吸电离飞行时间质谱对meso-四(对烷氧苯基)卟啉金属银配合物进行了表征.样品溶解在氯仿中,以正离子方式记录谱图,结果发现除了产生目标化合物分子离子峰外,没有任何碎片峰.激光解吸电离飞行时间质谱是表征这种meso-四(对烷氧苯基)卟啉金属银配合物有效的方法.
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| 关 键 词： | 卟啉金属配合物 激光解吸电离飞行时间质谱 meso-四(对烷氧苯基)卟啉 |
| 文章编号： | 1006-3757（2006）03-0158-03 |
| 收稿时间： | 2006-05-09 |
| 修稿时间： | 2006-07-06 |
Characterization of Silver Metallic Complexes of Meso-tetrakis (4-alkoxyphenyl) Porphyrins Using Laser Desorption Ionization Time-of-flight Mass Spectrometry (LDI-TOF-MS) |
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| JI Yi-ping,ZHANG Hong-ming and LIU Zi-yang.Characterization of Silver Metallic Complexes of Meso-tetrakis (4-alkoxyphenyl) Porphyrins Using Laser Desorption Ionization Time-of-flight Mass Spectrometry (LDI-TOF-MS)[J].Analysis and Testing Technology and Instruments,2006,12(3):158-160. |
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| Authors: | JI Yi-ping ZHANG Hong-ming and LIU Zi-yang |
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| Institution: | 1. Changchun Institute of Applied Chemistry, Chinese Academy of Sciences, Changchun 130022 ,China;2. Department of Chemistry, Zhejiang University, Hangzhou 310027, China |
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| Abstract: | A series of different structural silver metallic complexes of meso-tetrakis(4-alkoxyphenyl) porphyrins were characterized with laser desorption ionization time-of-flight mass spectrometry(LDI-TOF-MS) technique.The samples were dissolved in chloroform and the data were recorded by positive ion mode.No any other fragment was found except for little molecular fragment ion peaks.LDI-TOF-MS is very effective for the analysis of the novel metallic complexes of meso-tetrakis(4-alkoxyphenyl) porphyrins. |
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| Keywords: | metallic complexes of porphyrins laser desorption ionization time-of-flight mass spectrometry(LDI-TOF-MS) meso-tetrakis(4-alkoxyphenyl) porphyrins |
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