The method of flash vacuum pyrolysis,preparative applications and analytical studies |
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| Affiliation: | 1. Department of Polymer Technology, Kamaraj College of Engineering and Technology, S.P.G.C. Nagar, K. Vellakulam, Tamil Nadu 625 701, India;2. Radiation Technology Development Section, Bhabha Atomic Research Centre, Mumbai 400085, India;1. Center for Environmentally Beneficial Catalysis, University of Kansas, Lawrence, KS 66047, United States;2. Department of Chemistry, Iowa State University, Ames, IA 50011, United States;1. Generic Drug Research Center of Guizhou Province, School of Pharmacy, Zunyi Medical University, Zunyi 563000, PR China;2. National Engineering Research Center of Chiral Drugs, Chengdu Institute of Organic Chemistry, Chinese Academy of Sciences, Chengdu 610041, PR China;1. ICG Montpellier–UMR 5253, Equipe AM2N, ENSCM, 8, Rue de l''Ecole Normale, 34296 Montpellier CEDEX 5, France;2. Université Mentouri-Constantine, Département de chimie, Laboratoire d’Obtention de Substances Thérapeutiques (LOST), Campus Chaabet Ersas, 25000 Constantine, Algeria;3. Université Paris 13, Sorbonne Paris Cité, CSPBAT, CNRS UMR 7244, 74, Rue Marcel Cachin, F-93017 Bobigny, France;4. INSERM U-1051, Institut des Neurosciences de Montpellier, 80 Rue Augustin Fliche, 34091 Montpellier, France;5. Institut Européen des Membranes, cc047 Université de Montpellier 2, 34095 Montpellier, France;1. Department of Chemistry, Renmin University of China, Beijing 100872, PR China;2. College of Chemistry, Beijing Normal University, Beijing 100875, PR China |
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| Abstract: | Flash vacuum pyrolysis has been used to prepare a variety of differently substituted derivatives of the benzocyclobutene ring system starting with simple precursors. An analytical gas flow reactor is described which simulates reaction conditions of flash vacuum pyrolysis experiments. This reactor allows to optimise reaction conditions and to obtain structure reactivity correlations for thermolytic gas phase reactions. |
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