Reaction calorimetry for the development of chemical reactions |
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| Institution: | 1. Research and Development, Molekule Inc, 3802 Spectrum Blvd., Tampa, FL 33612, USA;2. Clean Energy Research Center, Department of Chemical, Biological and Materials Engineering, University of South Florida, 3820 Spectrum Blvd, Tampa, FL 33612, USA;3. Department of Chemistry, Sri Guru Teg Bahadur Khalsa College, Anandpur Sahib, Punjab 140118, India;4. CICECO – Aveiro Institute of Materials, Department of Chemistry, University of Aveiro, Aveiro 3810-193, Portugal;1. Mary Kay O’Connor Process Safety Center, Artie McFerrin Department of Chemical Engineering, Texas A&M University, College Station, TX 77843-3122, United States;2. University of Bologna, DICAM, Via Terracini 28, 40120 Bologna, Italy;3. Mary Kay O’Connor Process Safety Center at Qatar, Texas A&M University at Qatar, PO Box 23874, Education City, Doha, Qatar;1. LATA2M, Laboratoire de Thermodynamique Appliquée et Modélisation Moléculaire, University of Tlemcen, Post Office Box 119, Tlemcen 13000, Algeria;2. Laboratoire Multimatériaux et Interfaces, UMR 5615, Université de Lyon, Université Claude Bernard Lyon1, 69622 Villeurbanne, France;3. Université de Saint Etienne, Jean Monnet, F-42023 Saint Etienne, Université de Lyon, F-42023 Saint Etienne, France;4. Thermodynamics Research Unit, School of Engineering, University of KwaZulu-Natal, Howard College Campus, King George V Avenue, 4041 Durban, South Africa;1. Laboratoire Interdisciplinaire Carnot de Bourgogne (ICB), UMR 6303 CNRS / Université de Bourgogne Franche-Comté, 12 rue de la fonderie, 71200 Le Creusot, France;2. ArcelorMittal, 1 route de Saint Leu, 60761 Montataire, France;1. Chemistry Department, Moscow State University, 119992 Moscow, Russia;2. A.N. Nesmeyanov Institute of Organoelement Compounds of Russian Academy of Sciences (INEOS RAS), 119991 Moscow, Russia;3. Chemistry Department, Kazan State Technical University, 420008 Kazan, Russia |
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| Abstract: | A new reaction calorimeter is described that has been developed to study chemical reaction processes on a laboratory scale. It provides precise measurements of kinetic and thermal data, of heat transfer data, as well as of the physical properties of the reaction product. The reaction calorimeter is applied successfully in the development of chemical processes, in the evaluation of hazards and risks of chemical synthesis.Working principles and evaluation are described using the example of the nitration of benzaldehyde. |
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