Synthesis and fluorination of nitro-substituted thionocarbonates |
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Authors: | L. T. Eremenko G. V. Oreshko M. A. Fadeev |
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Affiliation: | (1) Institute of Chemical Physics in Chernogolovka, Russian Academy of Sciences, 142432 Chernogolovka, Moscow Region, Russian Federation |
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Abstract: | Thiocarbonylchloride reacts with -nitroalcohols yielding symmetrical thionocarbonates. Transesterification of bis(2-fluoro-2,2-dinitroethyl)thioncarbonate affords alkyl 2-fluoro-2,2-dinitroethylthionocarbonates. Fluorination of these thionocarbonates yields the corresponding difluoroformals.Translated fromIzvestiya Akademii Nauk. Seriya Khimicheskaya, No. 2, pp. 375–376, February, 1993. |
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Keywords: | thionocarbonates, nitro-substituted, synthesis fluorination difluoroformals, /content/gl5p220367862547/xxlarge946.gif" alt=" beta" align=" MIDDLE" BORDER=" 0" >-nitro-substituted |
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