An efficient protocol for the preparation of MOM ethers and their deprotection using zirconium(IV) chloride |
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| Authors: | G.V.M. Sharma K. Laxma Reddy P. Sree Lakshmi Palakodety Radha Krishna |
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| Affiliation: | D-211, Discovery Laboratory, Organic Chemistry Division III, Indian Institute of Chemical Technology, Hyderabad 500 007, India |
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| Abstract: | An efficient protocol for the preparation of MOM ethers from alcohols and formaldehyde dimethyl acetal (DMFA) using ZrCl4 (10 mol %) at room temperature under solvent free conditions has been developed. Similarly, the same Lewis acid, ZrCl4 (50 mol %), in isopropanol at reflux was utilised for the deprotection of MOM ethers. |
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| Keywords: | MOM ethers Formaldehyde dimethyl acetal Zirconium chloride |
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