Polymer-directed synthesis and magnetic property of nanoparticles-assembled BiFeO3 microrods |
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Authors: | Lei Zhang Ying-Li Ma Zi-Ling Xue |
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Affiliation: | a State Key Laboratory of Coordination Chemistry, Nanjing National Laboratory of Microstructures, School of Chemistry and Chemical Engineering, Nanjing University, Nanjing 210093, PR China b Department of Chemistry, The University of Tennessee, Knoxville, TN 37996-1600, USA |
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Abstract: | Nanoparticles-assembled BiFeO3 microrods were successfully prepared via a polymer-directed solvothermal route. The phase and morphology of the products were characterized by powder X-ray diffraction (XRD), energy dispersive spectrometry (EDS), inductively coupled plasma atomic emission spectroscopy (ICP-AES), FT-IR spectroscopy and scanning electron microscopy (SEM). Experiments indicated that the linking effect originated from the interactions between polymer molecules could direct the self-assembly of building blocks into one-dimensional nanoparticles-assembled BiFeO3 microrods. Some factors influencing the morphologies of the products were systematically investigated and a possible mechanism of the formation of the microrods was suggested. Moreover, the magnetic properties of the products were studied. |
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Keywords: | Oxide materials Microstructure Magnetic measurements |
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