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Microwave synthesis of secondary phosphines and phosphine oxides from red phosphorus and allyl(methoxy)benzenes in KOH-DMSO
Authors:V A Kuimov  S F Malysheva  A V Artem’ev  S O Kenzhetaeva  N A Belogorlova  T N Komarova  N K Gusarova  B A Trofimov
Institution:1. Favorskii Irkutsk Institute of Chemistry, Siberian Branch, Russian Academy of Sciences, ul. Favorskogo 1, Irkutsk, 664033, Russia
Abstract:Bis1-(methoxyphenyl)propan-2-yl]phosphines and bis1-(methoxyphenyl)propan-2-yl]phosphine oxides were synthesized by phosphorylation of allyl(methoxy)benzenes in the system red phosphorus-KOH · 0.5 H2O-DMSO under microwave irradiation.
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