Solid state hydrolysis/polycondensation of alkoxysilane: access to crystal-like silicon-based hybrid materials |
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Authors: | Muramatsu Hironobu Corriu Robert Boury Bruno |
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Affiliation: | UMR 5637, Laboratoire de Chimie moléculaire et organisation du solide, cc007, Université de Montpellier II, Place E. Bataillon, 34090 Montpellier, France. |
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Abstract: | Transformation of a crystallized molecular solid to a periodically organized covalent extended solid was obtained by a solvent-free process of an organosilane. Hydrolysis and further polycondensation occur in the solid state; in addition this route leads to crystal-like silicon-based hybrid materials with a higher periodicity than material prepared by sol-gel process. |
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