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Europium Luminescent Polymeric Microspheres Fabricated by Spray Drying Process
Authors:Priscilla Paiva Luz  Ana Maria Pires  Osvaldo Antonio Serra
Affiliation:1. Department of Chemistry, FFCLRP, University of S?o Paulo, Ribeir?o Preto, SP, Brazil
2. Department of Physics, Chemistry and Biology, FCT-UNESP, Presidente Prudente, SP, Brazil
3. Department of Chemistry, Rare Earth Laboratory, University of S?o Paulo, Av. Bandeirantes, 3900, 14040-901, Ribeir?o Preto, SP, Brazil
Abstract:The spray drying method was used to prepare luminescent microspheres. These microspheres were prepared by spraying an aqueous solution of dextrin and an europium(III) complex with subsequent drying in a hot medium. The spray dried powder was characterized by scanning electron microscopy (SEM) and photoluminescence spectroscopy (PL). Particle size distribution was estimated from SEM images. The ultrasonic spray drying technique was successfully applied to yield a microparticulated and red luminescent powder composed by the [Eu(dpa)(3)](3-) (dpa = dipicolinic acid) complex incorporated in dextrin microspheres.
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