Characterization of Fe and Fe50Ni50 ultrafine nanoparticles synthesized by inert gas-condensation method |
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Authors: | A. Djekoun N. Boudinar A. Otmani B. Bouzabata |
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Affiliation: | a Laboratoire de Magnétisme et de Spectroscopie des Solides Université Badji-Mokhtar, Faculté des Sciences, BP: 12 (23000) Annaba, Algeria b Laboratoire de Physique de l’Etat Condensé, UMR CNRS 6087 Université du Maine Faculté des Sciences, 72085 Le Mans Cedex 9, France |
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Abstract: | Nanoparticles of Fe and Fe50Ni50 were synthesized by inert gas-condensation method under pure helium atmosphere. The prepared nanoparticles samples were examined by high-resolution transmission electron microscopy, X-ray diffraction and Mössbauer spectroscopy. The synthesized nanoparticles consisted of core-shell type structure nearly spherical shape with a size comprised within the range 4-70 nm and they occur as clusters or chains. The Mössbauer measurements as well as X-ray diffraction showed, in both cases, the presence of iron-oxide phases. |
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Keywords: | 75.50.Bb 61.46.Df 61.10.Nz 68.37.Lp 76.80.+y |
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