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A highly efficient reaction of thiobenzophenone for 1-diazoalkene
Authors:Wataru Ando  Toshiya Furuhata  Toshikazu Takata
Affiliation:Department of Chemistry, The University of Tsukuba Sakura-mura, Ibaraki 305, Japan
Abstract:9-(Diazomethylene)fluorene formed in situ in the reaction of 9-(aminomethylidene)fluorene with n-butylnitrite, was successfully trapped by thiobenzophenone to afford 1,3,4-thiadiazoline derivative which was confirmed by spectroscopic and analytical data.
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