A highly efficient reaction of thiobenzophenone for 1-diazoalkene |
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Authors: | Wataru Ando Toshiya Furuhata Toshikazu Takata |
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Affiliation: | Department of Chemistry, The University of Tsukuba Sakura-mura, Ibaraki 305, Japan |
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Abstract: | 9-(Diazomethylene)fluorene formed in the reaction of 9-(aminomethylidene)fluorene with n-butylnitrite, was successfully trapped by thiobenzophenone to afford 1,3,4-thiadiazoline derivative which was confirmed by spectroscopic and analytical data. |
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