Synthese und Charakterisierung von 1,3-dithia-2-boryl-[3]ferrocenophanen |
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| Authors: | Dietmar Fest Carl D Habben |
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| Institution: | Institut für Anorganische Chemie der Universität Göttingen, Tammannstr. 4, D-3400 Göttingen F.R.G. |
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| Abstract: | The 1,3-dithia-2-boryl3]ferrocenophanes (I-VIII) are obtained from the reaction of ferrocene-1,1′-dithiol (A) with dihalogenorganylboranes by elimination of the hydrogenhalides. I-VIII can be also prepared by starting from Fe(C5H4SLi)2 · 2THF (B) inplace of A, but in lower yields. The air-sensitive 3] ferrocenophanes have been characterized analytically and spectroscopically (MS; NMR: 1H, 11B, 13C). |
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