Determination of liquid vapour adsorption and desorption on and from solids by means of the derivatograph II |
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Authors: | P Staszczuk |
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Institution: | (1) Department of Physical Chemistry, Institute of Chemistry, Maria Curie-Sk odovska University, M. Curie-Sk odovska SQ. 3, 20-031 Lublin, Poland |
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Abstract: | Studies of water adsorption and desorption on silica gel with a modified derivatograph are described. The dynamic gas chromatography step profile method was used to determine isotherms of adsorption and desorption from the TG curve. The obtained isotherms agree with those from other methods. The properties of surface liquid layers can be investigated by this method.
Zusammenfassung Die Untersuchung der Adsorption und Desorption von Wasser an Silikagel mittels eines modifizierten Derivatographen wird beschrieben. Die dynamische gaschromatographische Stufenprofilmethode wurde zur Bestimmung der Ad- und Desorptionsisothermen aus den TG-Kurven herangezogen. Die erhaltenen Isothermen stimmen gut mit denen nach anderen Methoden bestimmten überein. Die Eigenschaften flüssiger Oberflächenschichten können mit dieser Methode untersucht werden.
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