Synthesis and separation property of flower-like Cd(OH)2 microstructures via a simple solution route |
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Authors: | DongEn Zhang Qing Xie XiaoBo Zhang GuiQuan Han AiMei Chen |
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Affiliation: | a Department of Chemical Engineering, Huaihai Institute of Technology, Lianyungang 222005, PR China b Japan Science and Technology Agency (JST), Kawaguchi-shi, Saitama, Japan c Lianyungang Higher Vocational Technology College of Traditional Chinese Medicine, Lianyungang 222006, PR China |
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Abstract: | Well-defined flower-like Cd(OH)2 microstructures have been successfully synthesized via a simple aqueous solution route, using CdCl2 and NaOH as the reactants, and triethanolamine (TEA) as the modifying agent. X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM) and UV-vis spectrometer were used to characterize the products. SEM and TEM images illustrated that the flower-like Cd(OH)2 bundles consisted of hexagonal nanoplates with thickness of about 50 nm. The adsorption of TEA on (0 0 1) plane of the growing Cd(OH)2 crystal leads to the flower petals in appearance. Further experiments evidenced that the positively charged Cd(OH)2 could effectively adsorb or separate the negatively charged dye molecules. |
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Keywords: | Cd(OH)2 microstructures 3D flower-like Aqueous solution route Growth process |
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