A Novel Synthesis of Isothiocyanates from Amines Using Triphenylphosphine/Carbon Tetrachloride |
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| Authors: | Isao Furukawa Noboru Abe Shizunobu Hashimoto |
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| Institution: | Department of chemistry , Doshisha University , Karasuma-imadegawa, Kamigyo-ku, Kyoto , 602 , Japan |
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| Abstract: | Abstract Triethylammonium dithiocarbamates (RNHC (S) S.HNEt3), prepared from aliphatic and/or aromatic amines, carbon disulfide and triethylamine, were treated with triphenylphosphine/carbon tetrachloride to give the corresponding isothiocyanates in good yields. |
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