| 3-(3-叔丁氧基)丁二酰亚胺基单环β-内酰胺衍生物的合成 |
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| 引用本文： | 张萍,王萍,李媛. 3-(3-叔丁氧基)丁二酰亚胺基单环β-内酰胺衍生物的合成[J]. 有机化学, 2007, 27(8): 1031-1033 |
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| 作者姓名： | 张萍 王萍 李媛 |
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| 作者单位： | 1. 河北师范大学化学与材料科学学院,石家庄,050016
2. 河北师范大学化学与材料科学学院,石家庄,050016;河北化工医药职业技术学院化工系,石家庄,050012 |
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| 基金项目： | 河北省自然科学基金（No.B2004000145）资助项目. |
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| 摘 要： | 从苹果酸出发, 经过一系列反应得到3-(3-叔丁氧基)丁二酰亚胺乙酰氯. 3-(3-叔丁氧基)丁二酰亚胺乙酰氯和含不同取代基的Schiff碱1a～1h反应得到8个新的3-(3-叔丁氧基)丁二酰亚胺基单环β-内酰胺衍生物2a～2h, 化合物2a～2h的结构经IR, 1H NMR, MS和元素分析所确证.
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| 关 键 词： | 3-(3-叔丁氧基)丁二酰亚胺乙酰氯 Schiff碱 单环β-内酰胺 |
| 收稿时间： | 2006-06-20 |
| 修稿时间： | 2006-06-202007-01-22 |
Synthesis of New 3-(3-t-Butoxyl)succinimidyl Monocyclic β-Lactams |
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| ZHANG,Ping,WANG,Ping,LI,Yuan. Synthesis of New 3-(3-t-Butoxyl)succinimidyl Monocyclic β-Lactams[J]. Chinese Journal of Organic Chemistry, 2007, 27(8): 1031-1033 |
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| Authors: | ZHANG Ping WANG Ping LI Yuan |
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| Affiliation: | 1. College of Chemistry, Hebei Normal University, Shijiazhuang 050016; 2. Department of Chemistry and Enginering, Hebei Chemical and Pharmacutical Vocational Technology College, Shijiazhuan g 050012 |
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| Abstract: | 3-(3-t-Butoxyl)succinimidyl acetyl chloride was obtained by a series of reactions starting from malic acid. 3-(3-t-Butoxyl)succinimidyl acetyl chloride reacted with Schiff bases 1a～1h to yield 8 new 3-(3-t-butoxyl)succinimidyl monocyclic β-lactam derivatives 2a～2h. The structures of the new compounds were confirmed by IR, 1H NMR, MS spectra and elemental analysis. |
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| Keywords: | 3-(3-t-butoxyl)succinimide acetyl chloride Schiff base monocyclic β-lactam |
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