| 微波消解-氢化物发生原子荧光法测定天麻粉中的硒 |
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| 引用本文： | 汤进贤,黄锋. 微波消解-氢化物发生原子荧光法测定天麻粉中的硒[J]. 广东微量元素科学, 2009, 16(8): 49-51 |
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| 作者姓名： | 汤进贤 黄锋 |
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| 作者单位： | 昭通市疾病预防控制中心,云南,昭通,657000;昭通市疾病预防控制中心,云南,昭通,657000 |
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| 摘 要： | 为建立测定天麻粉中硒的方法，采用微波消解技术溶解天麻粉，利用原子荧光法在优化条件下测定了其中硒的含量。结果表明，测定天麻中硒的回收率为93．1％～103．5％，RSD为4．5％。该法具有检出限低、灵敏度高、简便、准确、快速、线性范围宽等特点，能够达到测定天麻中微量硒的要求。
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| 关 键 词： | 天麻粉 微波消解 原子荧光光谱法 硒 |
Determination of Selenium in Gastrodia Powder by Atomic Flurescence Spectrometry with Microwave Digestion |
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| TANG Jinxian,HUANG Feng. Determination of Selenium in Gastrodia Powder by Atomic Flurescence Spectrometry with Microwave Digestion[J]. Trace Elements Science, 2009, 16(8): 49-51 |
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| Authors: | TANG Jinxian HUANG Feng |
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| Affiliation: | TANG Jinxian,HUANG Feng(Zhaotong Centers for Disease Prevention and Control,Yunnan Zhaotong 657000,China) |
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| Abstract: | To establish a method for determination of selenium in Gastrodia Powder, atomic fluorescence spectrometer was applied to determine selenium under optimized conditions in Gastrodia, microwave digestion was employed in sample pretreatment. The results show that the precision and recovery of Selenium in gastrodia are between 93.1% - 103.5% and between 4. 5%. It indicates that the methods can be applied to determine selenium in Gastrodia Powder with simple, fast and accurate. |
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| Keywords: | Gastrodia Powder micro-wave digestion atomic fluorescence spectrometry selenium |
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