| 1-(2,6-二氟苯甲基)-N-甲基-1H-1,2,3-三唑-4-甲酰胺核磁共振峰的归属 |
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| 引用本文： | 王思宏,尹秀梅.1-(2,6-二氟苯甲基)-N-甲基-1H-1,2,3-三唑-4-甲酰胺核磁共振峰的归属[J].分析化学,2006,34(3):362-364. |
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| 作者姓名： | 王思宏 尹秀梅 |
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| 作者单位： | 1. 延边大学分析测试中心,延吉,133002
2. 延边大学药学院,延吉,133000 |
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| 摘 要： | 采用一维(1D)和二维(2D)核磁共振(NMR)技术对一种抗癫痫活性的化合物1-(2,6-二氟苯甲基)-N-甲基-1H-1,2,3-三唑-4甲酰胺的1H和13C NMR信号进行了归属。
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| 关 键 词： | 核磁共振 1 2 3-三唑 抗癫痫 归属 |
| 收稿时间： | 04 22 2005 12:00AM |
| 修稿时间： | 2005-04-222005-08-24 |
Assignments of Nuclear Magnetic Resonance Peak of 1-(2,6-Difiurophenymethyl) -N-methyl-1 H-1, 2,3-Triazole- 4-carboxamide |
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| Wang Sihong,Yin Xiumei.Assignments of Nuclear Magnetic Resonance Peak of 1-(2,6-Difiurophenymethyl) -N-methyl-1 H-1, 2,3-Triazole- 4-carboxamide[J].Chinese Journal of Analytical Chemistry,2006,34(3):362-364. |
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| Authors: | Wang Sihong Yin Xiumei |
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| Institution: | 1.Center of Analysis and Test, Yanbian University, Yanji 133002;2.College of Pharmacy, Yanbian University, Yanji 133000 |
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| Abstract: | The H-H correlated spectroscopy (H-H COSY), distortionless enhancement by polartization transfer spectrum (DEPT), heteronuclear multiple bond correlation (HMBC) and heteronuclear multiple quantum correlation (HMQC) spectra of 1-(2,6-diflurophenymethyl)-N-methyl-1H-1,2,3-triazole- 4-carboxamide which is a class of antiepileptic agent were reported and interpreted. All the ~1H nuclear magnetic resonance (NMR) and ~ 13 C NMR chemical shifts were assigned by means of ~1H- ~1H COSY, HMQC, DEPT-135 and HMBC . |
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| Keywords: | Nuclear magnetic resonance 1 2 3-triazole antiepileptic assignment |
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