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Epsilon5高能偏振能量色散X-射线荧光光谱仪测定垃圾焚烧灰渣中有害元素
引用本文:张勤,李国会,吉昂,李小莉,张斌生. Epsilon5高能偏振能量色散X-射线荧光光谱仪测定垃圾焚烧灰渣中有害元素[J]. 分析试验室, 2010, 29(4)
作者姓名:张勤  李国会  吉昂  李小莉  张斌生
作者单位:中国地质科学院地球物理地球化学勘查研究所,廊坊,065000;上海硅酸盐研究所,上海,200050;天津地质矿产研究所,天津,300000;广州珠江水泥厂,广州,510460
摘    要:使用粉末样品压片制样,用Epsilon5高能偏振能量色散X射线荧光(EDXRF)光谱仪测定垃圾焚烧灰渣中S、Cl、Ba、Cr、Cu、Na、Mn、Pb、Zn、Cd、As、Mo等多种有害元素,采用土壤、水系沉积物、海底沉积物、矿物等国家标准物质和人工合成标样作为校准。

关 键 词:高能偏振EDXRF光谱仪  垃圾焚烧灰渣  粉末样品压片  多元素同时分析

Determination of many harmful elements in ash sludge for refuse incineration by epsilon5 high-energy polarized-beam EDXRF
ZHANG Qin,LI Guo-hui,JI Ang,LI Xiao-li,ZHANG Bin-sheng. Determination of many harmful elements in ash sludge for refuse incineration by epsilon5 high-energy polarized-beam EDXRF[J]. Chinese Journal of Analysis Laboratory, 2010, 29(4)
Authors:ZHANG Qin  LI Guo-hui  JI Ang  LI Xiao-li  ZHANG Bin-sheng
Affiliation:1.Institute of Geophysical and Geochemical Exploration;Chinese Academy of Geological Sciences;Langfang 065000;2.Shanghai Institute of Ceramics;Chinese Academy of Sciences;Shanghai 200050;3.Tianjin Institute of Geology and Mineral;Tianjin 300000;4.Guangzhou Zhujiang Cement Factory;Guangzhou 510460
Abstract:Many harmful elements including Ag,Ba,Cr,Cu,Ni,Mn,Pb,Zn,Cd,Se,As and Mo etc in the ash sludge for refuse incineration have been determined by pressed powder pellets using epsilon5 high-energy polarized-beam EDRXF spectrometer.The calibration curves were prepared using the soils,stream sediment,marine sediment and ore of multi-national certified reference material and synthetic standard.The method provides the advantages of simple operation and high efficiency.The precision and accuracy of the method can mee...
Keywords:High-energy polarized-beam EDXRF spectrometer  Ash sludge for refine incineration  Pressed powder pellets  Simultaneous measurement of multi-elements  
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