Crystal and molecular structure of (exo)-2-phenyl-5-ethoxycarbonyl-4,5,6,11b-tetrahydroisoxazolidino-[2,3-a]-β-carboline,C22H22N2O3期刊界 All Journals 搜尽天下杂志传播学术成果专业期刊搜索期刊信息化学术搜索

按检索

Crystal and molecular structure of (exo)-2-phenyl-5-ethoxycarbonyl-4,5,6,11b-tetrahydroisoxazolidino-[2,3-a]-β-carboline,C22H22N2O3

Authors:	J M M Smits P T Beurskens R Plate H C J Ottenheijm

Institution:	(1) Crystallography Laboratory, University of Nijmegen, Toernooiveld, 6525 ED Nijmegen, The Netherlands;(2) Department of Organic Chemistry, University of Nijmegen, Toernooiveld, 6525 ED Nijmegen, The Netherlands

Abstract:	The structure of the title compound, C₂₂H₂₂N₂O₃, was determined by X-rays atT=290 K.M _r=362.427, orthorombic, space groupPbca,a=11.666(4),b=15.691(1),c=20.931(1) Å,V=3831.4 Å³,Z=8,D _x=1.257 Mgm^–3. CuK radiation (graphite crystal monochromator, =1.54178 Å),(CuK)=6.42 cm^–1. Final conventionalR-factor=0.050,R _w=0.062 for 2552 observed reflections and 301 variables. The structure was solved usingMultan.

Keywords:
本文献已被 SpringerLink 等数据库收录！