Investigation on the thermal behaviour of Mg(NO3)2·6H2O |
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Authors: | R Naumann H -H Emons K Köhnke J Paulik F Paulik |
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Institution: | (1) Sektion Chemie, Bergakademie Freiberg, 9200 Freiberg, G.D.R.;(2) Institute of General and Analytical Chemistry, Technical University, Budapest, Hungary |
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Abstract: | DTA, DSC and X-ray investigations of Mg(NO3)2 · 6H2O revealed a lattice transformation at (71±2) C with H=12.5 J/g, and congruent melting at 90 C with H=150.3 J/g. The results of the DTA investigations on different Mg(NO3)2-H2O samples are in good agreement with those of solubility investigations. The melting enthalpy of Mg(NO3)3 · 6H2O is lowered considerably by deviation from the stoichiometric water content of the compound. The results allow conclusions as to the application of this salt hydrate as a latent heat-storage material.
Zusammenfassung DTA-, DSC- und röntgenographische Untersuchungen von Mg(NO3)2 · 6H2O zeigten die Existenz einer Gitterumwandlung bei (71±2) C mit H=12.5 J/g und ein kongruentes Schmelzen bei 90 C mit H=150.3 J/g. Die Ergebnisse der DTA-Untersuchungen an verschiedenen Mg(NO3)2-H2O Proben stehen in guter übereinstimmung mit denen von Löslichkeitsuntersuchungen. Durch ein Abweichen vom stöchiometrischen Wassergehalt der Verbindung wird die Schmelzenthalpie von Mg(NO3)2 · 6H2O beträchtlich vermindert. Die Ergebnisse ermöglichen Aussagen zur Anwendbarkeit dieses Salzhydrates als Wärmespeichermedium.
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![Ocy](/content/w63q6g6r13718728/xxlarge1054.gif) ![Dcy](/content/w63q6g6r13718728/xxlarge1044.gif) ![Ocy](/content/w63q6g6r13718728/xxlarge1054.gif) ![scy](/content/w63q6g6r13718728/xxlarge1089.gif) ![tcy](/content/w63q6g6r13718728/xxlarge1090.gif) ![IEcy](/content/w63q6g6r13718728/xxlarge1045.gif) ![khcy](/content/w63q6g6r13718728/xxlarge1093.gif) ![Icy](/content/w63q6g6r13718728/xxlarge1048.gif) ![Ocy](/content/w63q6g6r13718728/xxlarge1054.gif) ![Mcy](/content/w63q6g6r13718728/xxlarge1052.gif) ![IEcy](/content/w63q6g6r13718728/xxlarge1045.gif) ![tcy](/content/w63q6g6r13718728/xxlarge1090.gif) ![Rcy](/content/w63q6g6r13718728/xxlarge1056.gif) ![Icy](/content/w63q6g6r13718728/xxlarge1048.gif) ![IEcy](/content/w63q6g6r13718728/xxlarge1045.gif) ![scy](/content/w63q6g6r13718728/xxlarge1089.gif) ![kcy](/content/w63q6g6r13718728/xxlarge1082.gif) ![Ocy](/content/w63q6g6r13718728/xxlarge1054.gif) ![gcy](/content/w63q6g6r13718728/xxlarge1075.gif) . ![Rcy](/content/w63q6g6r13718728/xxlarge1056.gif) ![IEcy](/content/w63q6g6r13718728/xxlarge1045.gif) ![zhcy](/content/w63q6g6r13718728/xxlarge1078.gif) ![Ucy](/content/w63q6g6r13718728/xxlarge1059.gif) ![lcy](/content/w63q6g6r13718728/xxlarge1083.gif) ![softcy](/content/w63q6g6r13718728/xxlarge1100.gif) ![tcy](/content/w63q6g6r13718728/xxlarge1090.gif) ![Acy](/content/w63q6g6r13718728/xxlarge1040.gif) ![tcy](/content/w63q6g6r13718728/xxlarge1090.gif) ![pcy](/content/w63q6g6r13718728/xxlarge1087.gif) ![Ocy](/content/w63q6g6r13718728/xxlarge1054.gif) ![Vcy](/content/w63q6g6r13718728/xxlarge1042.gif) ![IEcy](/content/w63q6g6r13718728/xxlarge1045.gif) ![Dcy](/content/w63q6g6r13718728/xxlarge1044.gif) ![IEcy](/content/w63q6g6r13718728/xxlarge1045.gif) ![Ncy](/content/w63q6g6r13718728/xxlarge1053.gif) ![Ncy](/content/w63q6g6r13718728/xxlarge1053.gif) ![ycy](/content/w63q6g6r13718728/xxlarge1099.gif) ![Icy](/content/w63q6g6r13718728/xxlarge1048.gif) ![scy](/content/w63q6g6r13718728/xxlarge1089.gif) ![scy](/content/w63q6g6r13718728/xxlarge1089.gif) ![lcy](/content/w63q6g6r13718728/xxlarge1083.gif) ![IEcy](/content/w63q6g6r13718728/xxlarge1045.gif) ![Dcy](/content/w63q6g6r13718728/xxlarge1044.gif) ![Ocy](/content/w63q6g6r13718728/xxlarge1054.gif) ![Vcy](/content/w63q6g6r13718728/xxlarge1042.gif) ![Acy](/content/w63q6g6r13718728/xxlarge1040.gif) ![Ncy](/content/w63q6g6r13718728/xxlarge1053.gif) ![Icy](/content/w63q6g6r13718728/xxlarge1048.gif) ![pcy](/content/w63q6g6r13718728/xxlarge1087.gif) ![Ocy](/content/w63q6g6r13718728/xxlarge1054.gif) ![zhcy](/content/w63q6g6r13718728/xxlarge1078.gif) ![Vcy](/content/w63q6g6r13718728/xxlarge1042.gif) ![Ocy](/content/w63q6g6r13718728/xxlarge1054.gif) ![Icy](/content/w63q6g6r13718728/xxlarge1048.gif) ![lcy](/content/w63q6g6r13718728/xxlarge1083.gif) ![scy](/content/w63q6g6r13718728/xxlarge1089.gif) ![Dcy](/content/w63q6g6r13718728/xxlarge1044.gif) ![IEcy](/content/w63q6g6r13718728/xxlarge1045.gif) ![lcy](/content/w63q6g6r13718728/xxlarge1083.gif) ![Acy](/content/w63q6g6r13718728/xxlarge1040.gif) ![tcy](/content/w63q6g6r13718728/xxlarge1090.gif) ![zhcy](/content/w63q6g6r13718728/xxlarge1078.gif) ![Acy](/content/w63q6g6r13718728/xxlarge1040.gif) ![kcy](/content/w63q6g6r13718728/xxlarge1082.gif) ![lcy](/content/w63q6g6r13718728/xxlarge1083.gif) ![Ucy](/content/w63q6g6r13718728/xxlarge1059.gif) ![CHcy](/content/w63q6g6r13718728/xxlarge1063.gif) ![IEcy](/content/w63q6g6r13718728/xxlarge1045.gif) ![Ncy](/content/w63q6g6r13718728/xxlarge1053.gif) ![Icy](/content/w63q6g6r13718728/xxlarge1048.gif) ![pcy](/content/w63q6g6r13718728/xxlarge1087.gif) ![Ocy](/content/w63q6g6r13718728/xxlarge1054.gif) ![tcy](/content/w63q6g6r13718728/xxlarge1090.gif) ![IEcy](/content/w63q6g6r13718728/xxlarge1045.gif) ![Ncy](/content/w63q6g6r13718728/xxlarge1053.gif) ![tscy](/content/w63q6g6r13718728/xxlarge1094.gif) ![Acy](/content/w63q6g6r13718728/xxlarge1040.gif) ![lcy](/content/w63q6g6r13718728/xxlarge1083.gif) ![softcy](/content/w63q6g6r13718728/xxlarge1100.gif) ![Ncy](/content/w63q6g6r13718728/xxlarge1053.gif) ![Ocy](/content/w63q6g6r13718728/xxlarge1054.gif) ![pcy](/content/w63q6g6r13718728/xxlarge1087.gif) ![Rcy](/content/w63q6g6r13718728/xxlarge1056.gif) ![Icy](/content/w63q6g6r13718728/xxlarge1048.gif) ![Mcy](/content/w63q6g6r13718728/xxlarge1052.gif) ![IEcy](/content/w63q6g6r13718728/xxlarge1045.gif) ![Ncy](/content/w63q6g6r13718728/xxlarge1053.gif) ![IEcy](/content/w63q6g6r13718728/xxlarge1045.gif) ![Ncy](/content/w63q6g6r13718728/xxlarge1053.gif) ![Icy](/content/w63q6g6r13718728/xxlarge1048.gif) ![IOcy](/content/w63q6g6r13718728/xxlarge1025.gif) ![Ocy](/content/w63q6g6r13718728/xxlarge1054.gif) ![scy](/content/w63q6g6r13718728/xxlarge1089.gif) ![Ocy](/content/w63q6g6r13718728/xxlarge1054.gif) ![lcy](/content/w63q6g6r13718728/xxlarge1083.gif) ![kcy](/content/w63q6g6r13718728/xxlarge1082.gif) ![Acy](/content/w63q6g6r13718728/xxlarge1040.gif) ![CHcy](/content/w63q6g6r13718728/xxlarge1063.gif) ![IEcy](/content/w63q6g6r13718728/xxlarge1045.gif) ![scy](/content/w63q6g6r13718728/xxlarge1089.gif) ![tcy](/content/w63q6g6r13718728/xxlarge1090.gif) ![Vcy](/content/w63q6g6r13718728/xxlarge1042.gif) ![tcy](/content/w63q6g6r13718728/xxlarge1090.gif) ![IEcy](/content/w63q6g6r13718728/xxlarge1045.gif) ![pcy](/content/w63q6g6r13718728/xxlarge1087.gif) ![lcy](/content/w63q6g6r13718728/xxlarge1083.gif) ![Ocy](/content/w63q6g6r13718728/xxlarge1054.gif) ![Vcy](/content/w63q6g6r13718728/xxlarge1042.gif) ![Ocy](/content/w63q6g6r13718728/xxlarge1054.gif) ![gcy](/content/w63q6g6r13718728/xxlarge1075.gif) ![kcy](/content/w63q6g6r13718728/xxlarge1082.gif) ![kcy](/content/w63q6g6r13718728/xxlarge1082.gif) ![Ucy](/content/w63q6g6r13718728/xxlarge1059.gif) ![Mcy](/content/w63q6g6r13718728/xxlarge1052.gif) ![Ucy](/content/w63q6g6r13718728/xxlarge1059.gif) ![lcy](/content/w63q6g6r13718728/xxlarge1083.gif) ![softcy](/content/w63q6g6r13718728/xxlarge1100.gif) ![tcy](/content/w63q6g6r13718728/xxlarge1090.gif) ![Ocy](/content/w63q6g6r13718728/xxlarge1054.gif) ![Rcy](/content/w63q6g6r13718728/xxlarge1056.gif) .
We thank Dr. Flammersheim, Department of Chemistry, FSU, Jena, for the DSC measueements. |
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