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Syntheses, structures, and properties of the Co(II), Ni(II), and Cu(II) complexes with 5-carboxy- and 5-methoxycarbonylpyrazoles |
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| Authors: | O. G. Shakirova L. G. Lavrenova N. V. Kuratieva D. Yu. Naumov A. S. Bogomyakov L. A. Sheludyakova T. F. Mikhailovskaya S. F. Vasilevsky |
| Affiliation: | 1. Nikolaev Institute of Inorganic Chemistry, Siberian Branch, Russian Academy of Sciences, pr. akademika Lavrent??eva 3, Novosibirsk, 630090, Russia 2. Novosibirsk State University, Novosibirsk, Russia 3. International Tomography Center, Siberian Branch, Russian Academy of Sciences, Novosibirsk, Russia 4. Institute of Chemical Kinetics and Combustion, Siberian Branch, Russian Academy of Sciences, Novosibirsk, Russia |
| Abstract: | New cobalt(II), nickel(II), and copper(II) complexes based on 5-methoxycarbonyl-3-me-thylpyrazole (MePzCOOMe), [Co(MePzCOOMe)2(H2O)2](NO3)2 (I), [Ni(MePzCOOMe)2(H2O)2] (NO3)2 (II), and [Cu(MePzCOO)2(H2O)] · 3H2O (III), were synthesized. The compounds were studied by X-ray diffraction analysis, IR spectroscopy, and static magnetic susceptibility. The molecular and crystal structures of complexes I and III were determined by X-ray structure analysis. |
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