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Synthesis and crystal structures of 1,2-diaminobenzene-Ni complexes |
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| Authors: | L. Mei L. S. Tai Z. S. Ming S. Jie L. Q. Rong |
| Affiliation: | 1. Hefei University of Technology, Hefei, 230009, P.R. China 2. University of Science and Technology of China, Hefei, 230009, P.R. China 3. Shanghai Institute of Organic Chemistry, Shanghai, 200032, P.R. China |
| Abstract: | Treatment in different proportions of 1,2-diaminobenzene with Ni(OAc)2 · 4H2O in methanol results in the formation of two 1,2-diaminobenzene-Ni complexes I (C92H134N24Ni9O28) and II (C16H22N4NiO4). Their structures were determined by X-ray diffraction analysis. The complexes are also characterized by elemental analysis and IR. |
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