Beitrag zur aufeinanderfolgenden thermochemischen Bestimmung von SiO2 und Al2O3 Aus flusssaurer lösung |
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Authors: | H Strauβ R Rutkowski J Brand?tetr I Sajó |
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Institution: | (1) Veb Chemische Fabrik Fährbrücke, 9513 Langenbach, DDR;(2) Lehrstuhl für Chemie, Technische Universität, 66 238 Brno, SSR;(3) Eisenforschungsinstitut, 1509 Budapest, Ungarn |
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Abstract: | Zusammenfassung Die vorliegende Arbeit gibt eingangs einen Überblick von Publikationen, die sich mit der thermochemischen Bestimmung von SiO2 und Al2O3 aus flußsaurer Lösung befassen. Davon ausgehend werden Versuche beschrieben und Ergebnisse diskutiert, die mit konstanten Einwaagen von 700 mg SiO2 und etwa 100 mg Al2O3 aus flußsaurer Lösung und verschiedenen Kombinationen von Injektionsreagenzien erhalten wurden und die auf die Belange der Analyse von gefällten Natriumaluminiumsilicaten abgestimmt waren. Die vorgenommenen Untersuchungen führen zu den Schluß, daß Al2O3 und SiO2 in Natriumaluminiumsilicaten aus flußsaurer Lösung mit der Injektionsreagenskombination SrCl2KCl bestimmt werden sollten.
The first part of the paper gives a review of the literature dealing with thermochemical determinations of SiO2 and Al2O3 in hydrofluoric acid solution. The results of experiments with constant samples weights of 700 mg SiO2 and about 100 mg Al2O3 in hydrofluoric acid solution with differently combined injection reagents are discussed. The determinations were based on the analysis of precipitated sodium aluminium silicates.The investigations revealed that combined SrCl2/KCl solution should be used as injection reagent for determination of the Al2O3 and SiO2 contents of sodium aluminium silicates in hydrofluoric acid.
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![dcy](/content/u702214rw03vr827/xxlarge1076.gif) ![ncy](/content/u702214rw03vr827/xxlarge1085.gif) ![ocy](/content/u702214rw03vr827/xxlarge1086.gif) ![kcy](/content/u702214rw03vr827/xxlarge1082.gif) ![icy](/content/u702214rw03vr827/xxlarge1080.gif) ![scy](/content/u702214rw03vr827/xxlarge1089.gif) ![lcy](/content/u702214rw03vr827/xxlarge1083.gif) ![ocy](/content/u702214rw03vr827/xxlarge1086.gif) ![tcy](/content/u702214rw03vr827/xxlarge1090.gif) .
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