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One-step synthesis of colloidal Mn3O4 and γ-Fe2O3 nanoparticles at room temperature
Authors:Shuijin Lei  Kaibin Tang  Zhen Fang  Jie Sheng
Affiliation:(1) School of Materials Science and Engineering, Nanchang University, Nanchang, Jiangxi, 330031, P. R. China;(2) Nanomaterial and Nanochemistry, Hefei National Laboratory for Physical Sciences at Micro-scale, University of Science and Technology of China, Hefei, Anhui, 230026, P. R. China
Abstract:A facile room-temperature synthesis has been developed to prepare colloidal Mn3O4 and γ-Fe2O3 nanoparticles (5 to 25 nm) by an ultrasonic-assisted method in the absence of any additional nucleation and surfactant. The morphology of the as-prepared samples was observed by transmission electron microscopy. High-resolution transmission electron microscopy observations revealed that the as-synthesized nanoparticles were single crystals. The magnetic properties of the samples were investigated with a superconducting quantum interference device magnetometer. The possible formation process has been proposed.
Keywords:one-step synthesis  colloidal nanoparticles  Mn3O4   γ  -Fe2O3   ultrasonic-assisted method  magnetic properties  metal oxide nanoparticles
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