Reaction of phenyldichlorophosphine with diacetyl |
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| Authors: | A. N. Pudovik V. K. Khairullin N. I. Kharitonova |
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| Affiliation: | (1) A.E. Arbuzov Institute of Organic and Physical Chemistry, Academy of Sciences of the USSR, USSR |
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| Abstract: | Conclusions Phenyldichlorophosphine reacts with diacetyl to form 5-methyl-2-phenyl-4-chloro-2-oxo-1,2-oxaphosphol-4-ene. Hydrolysis of this compound gives phenyl-( -chloro- -oxo)butylphosphinic acid, and alcoholysis gives the ester of this acid.Translated from Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, No. 2, pp. 466–468, February, 1969. |
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