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在火焰原子吸收光度计上以无火焰原子化法测定碱金属元素
引用本文:梁述忠,石亚平. 在火焰原子吸收光度计上以无火焰原子化法测定碱金属元素[J]. 化学分析计量, 2006, 15(5): 26-28
作者姓名:梁述忠  石亚平
作者单位:徐州工业职业技术学院,徐州,221002;江苏省机电研究所,徐州,221000
基金项目:江苏省高校自然科学基金
摘    要:在常规火焰原子吸收分光光度计上采用特制的不锈钢原子化管对碱金属元素进行无火焰原子化法测定,克服了碱金属元素在火焰中的电离效应,试液用量极少。测定结果的相对标准偏差小于0.3%(n=11),回收率为98.9%~99.2%。

关 键 词:原子吸收分光光度计  无火焰原子化器  不锈钢原子化管  碱金属元素
修稿时间:2006-07-06

DETERMINATION OF THE ALKALI METAL ELEMENTS BY THE NON -FLAME ATOMIZATION METHOD ON FLAME ATOMIC ABSORPTION SPECTROPHOTOMETER
Liang Shuzhong,Shi Yaping. DETERMINATION OF THE ALKALI METAL ELEMENTS BY THE NON -FLAME ATOMIZATION METHOD ON FLAME ATOMIC ABSORPTION SPECTROPHOTOMETER[J]. Chemical Analysis And Meterage, 2006, 15(5): 26-28
Authors:Liang Shuzhong  Shi Yaping
Abstract:The alkali metal elements were determined by the non-flame atomization method on tradition flame atomic absoption spectrophotometer which was installed special prepared stainless steel atomizing tube.Ionization effect of the alkali metal elements was completely overcomed.Little sample solution were used.The relative standard deviation of results were less than 0.3%(n=11) for five elements,and recoveries were 98.9%~99.2%.
Keywords:atomic absorption spectrophotometer  non-flame atomizer  stainless steel atomizing tube  alkali metal element  
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