Analytical aspects of some organic acids |
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Authors: | C S Pande and T S Srivastava |
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Institution: | (1) Chemistry Department, Lucknow University, Lucknow, India |
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Abstract: | Summary A direct complexometric titration of iron(III) with EDTA using o- and p-cresotic acids indicators is given. The colour change at the end point is from blue-violet to light yellow or colourless at low concentrations of iron(III)]. The optimum range of pH and temperature for carrying out the titrations is 1.99 to 4.2 and 35° to 55°C and 1.42 to 4.4 and 30° to 60° C, respectively. Iron(III) may easily and accurately be estimated in macro- and micro-gram quantities with the help of these metal indicators. Be, Mg, Ca, Sr, Ba, Cd, UO2 and Mn are without any interference in the estimation. Back titration procedures for determination of zirconium and thorium with iron(III) and o- and p-cresotic acids are carried out.Part V: See Z. analyt. Chem. 173, 196 (1960). |
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