1H and 13C assignments of five cembrenes from guggul |
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Authors: | Bai Shi Jain Mahendra |
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Institution: | Department of Chemistry and Biochemistry, University of Delaware, Newark, DE 19716, USA. bais@udel.edu |
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Abstract: | Chemical shift assignments of (1)H and (13)C of five cembrene compounds isolated from the hexane extract of guggul, the resin of Commiphora mukul, are reported. Using (1)H, (13)C, and 2D NMR methods their structures were determined as cembrene (1-isopropyl-4,8,12-trimethyl-cyclotetradeca-2,4,7,11-tetraene), cembrene A (1-isopropenyl-4,8,12-trimethyl-cyclotetradeca-4,8,12-triene), cembrenol (1-isopropyl-4,8,12-trimethyl-cyclotetradeca-3,7,11-trienol), mukulol (1-isopropyl-4,8,12-trimethyl- cyclotetradeca-3,7,11-trienol), and verticillol (4,8,12,15,15-pentamethyl-bicyclo9.3.1]pentadeca-3,7-dien-12-ol). |
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Keywords: | NMR 1H 13C cembrenes guggul |
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