An improved procedure for the palladium-catalyzed oxidative carbonylation of beta-amino alcohols to oxazolidin-2-ones |
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| Authors: | Gabriele Bartolo Mancuso Raffaella Salerno Giuseppe Costa Mirco |
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| Affiliation: | Dipartimento di Scienze Farmaceutiche, Università della Calabria, 87036 Arcavacata di Rende, Cosenza, Italy. b.gabriele@unical.it |
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| Abstract: | A highly efficient oxidative cyclocarbonylation of beta-amino alcohols and 2-aminophenol to oxazolidin-2-ones has been achieved by using PdI(2) in conjunction with KI as the catalytic system in DME under relatively mild conditions (100 degrees C and 20 atm of a 4:1 mixture of CO and air). |
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