| 2D-NMR对Phyllfofenone-A(Ⅰ)的~1H和~(13)C的完全指定 |
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| 引用本文： | 符雄,曾陇梅,苏镜娱. 2D-NMR对Phyllfofenone-A(Ⅰ)的~1H和~(13)C的完全指定[J]. 分析测试学报, 1992, 0(2) |
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| 作者姓名： | 符雄 曾陇梅 苏镜娱 |
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| 作者单位： | 中山大学化学系 广州(符雄，曾陇梅)，中山大学化学系 广州(苏镜娱) |
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| 基金项目： | 国家自然科学基金，国家教委博士点基金 |
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| 摘 要： | 采用多种二维NMR技术,并借助一维NOE差谱以及INAPT技术对新二倍半萜Phyllo-fenone-A(Ⅰ)的全部质子和碳信号进行了归属,并纠正了前人对其类似物的一些碳谱峰指定的错误。
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| 关 键 词： | 二维NMR 二倍半萜 相关 |
Complete ~(13)C, ~1H Assignments for Phyllofenone A(1) by Two Dimensional NMR |
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| Fu Xiong,Zeng Longmei,Su Jingyu. Complete ~(13)C, ~1H Assignments for Phyllofenone A(1) by Two Dimensional NMR[J]. Journal of Instrumental Analysis, 1992, 0(2) |
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| Authors: | Fu Xiong Zeng Longmei Su Jingyu |
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| Affiliation: | Fu Xiong,Zeng Longmei,Su Jingyu Department of Chemistry,Zhongshan University |
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| Abstract: | Various two dimensional NMR techniques, with the assistance of one dimensional differenceNOE and INAPT experiments, have been used to unambiguously assign ~1H and ~(13)C resonancesfor a new sesterterpene-phyllofenone A. Some assigning mistakes of ~(13)C data reportedpreviously have been corrected as well |
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| Keywords: | Two dimensional NMR Sesterterpene Correlation |
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